BIP! Finder - Cu(II), Ni(II) and Fe(III) complexes with 2′,2‴-(2,6-pyridindiyldiethylidene)-dioxamohydrazide in a monoanionic form. The crystal structure of aqua-2′,2‴-(2,6-pyridindiyldiethylidene)-dioxamohydrazidecopper(II) perchlorate

1998 • Cu(II), Ni(II) and Fe(III) complexes with 2′,2‴-(2,6-pyridindiyldiethylidene)-dioxamohydrazide in a monoanionic form. The crystal structure of aqua-2′,2‴-(2,6-pyridindiyldiethylidene)-dioxamohydrazidecopper(II) perchlorate

Authors: Ivana Ivanović-Burmazović, Alessia Bacchi, Giancarlo Pelizzi, Vukadin M. Leovac

Venue: Polyhedron

Type: Publication

Abstract: Abstract Starting from Cu(II) and Ni(II) perchlorate and Fe(III) chloride in the presence of 2,6-diacetylpyridine (dap) and semioxamazide (sox), the [Cu(Hdapsox)H 2 O]ClO 4 (I), [Ni(Hdapsox)(MeOH) 2 ]ClO 4 (II) and [Fe(Hdapsox)Cl 2 ] · 1 2 – H 2 O (III) complexes with a singly deprotonated ligand Hdapsox − of the acyl hydrazone class (with H 2 dapsox=2′,2‴-(2,6-pyridindiyldiethylidene)dioxamohydrazide) have been obtained and characterized for the first time by a template synthesis. The previously assumed [1] square-pyramidal structure ... (read more)

Topics: Crystallography Stereochemistry Inorganic chemistry

DOI: 10.1016/s0277-5387(98)00274-5

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